Experimental Organic Chemistry

Cranwell Philippa B. Experimental Organic Chemistry 3 ed. 2017 [pdf 907sc 47.97mb] 

The definitive guide to the principles and practice of experimental organic chemistry - fully updated and now featuring more than 100 experiments

The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures.

The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over 100 validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills.

New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry. New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis. Key aspects of this third edition include:

• Detailed descriptions of the correct use of common apparatus used in the organic laboratory
• Outlines of practical skills that all chemistry students must learn
• Highlights of aspects of health and safety in the laboratory, both in the first section and throughout the experimental procedures
• Four new sections reflecting advances in techniques and technologies, from electronic databases and information retrieval to semi-automated chromatography
• Mor